Optimized Process for Compressed Chewable Dietary Fiber Tablets Made of Pleurotus Geesteranus and Wheat Bran Powder
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摘要: 为优化秀珍菇麦麸膳食纤维咀嚼片粉末直接压片工艺的参数，以转台速度、充填深度和充填压力等单因素对产品综合评定值的影响作为研究对象，选取片质量差异、崩解时间、硬度和脆碎度作为综合评定评价指标，并通过响应面优化法确定其最佳工艺。结果表明，秀珍菇麦麸膳食纤维咀嚼片的最佳工艺为转台速度25 r·min-1、充填深度10 mm、充填压力24 kN，为麦麸膳食纤维资源的综合利用提供了科学理论依据。Abstract: A chewable dietary fiber tablet product made of wheat bran and mushroom (Pleurotus Geesteranus) powder by compression was studied. The rotational speed, filling depth and stowing pressure in compressing the ingredients were optimized against the weight deviation, disintegration time, hardness and friability of the tablets formedusing the response surface methodology. The optimized tablet formation was obtained with a rotational speed of 25 r·min-1 to make tablets of 10 mm thick under 24 kN stowing pressure.
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图 1 转台速度对秀珍菇麦麸膳食纤维咀嚼片综合评定值的影响
Figure 1. Effect of rotational speed on comprehensive evaluation of chewable P. geesteranus/wheat bran dietary fiber tablets
图 2 充填深度对秀珍菇麦麸膳食纤维咀嚼片综合评定值的影响
Figure 2. Effect of filling depth on comprehensive evaluation of chewable P. geesteranus/wheat bran dietary fiber tablets
图 3 充填压力对秀珍菇麦麸膳食纤维咀嚼片综合评定值的影响
Figure 3. Effect of stowing pressure on comprehensive evaluation of chewable P. geesteranus/wheat bran dietary fiber tablets
图 4 转台速度和充填压力对综合评定值的交互影响
Figure 4. Response surface plot for interactive effect of rotational speed and stowing pressure on comprehensive evaluation
图 5 充填深度和充填压力对综合评定值的交互影响
Figure 5. Response surface plot for interactive effect of filling depth and stowing pressure on comprehensive evaluation
表 1 响应面试验因素与水平
Table 1. Code and level of independent variables in Box-Behnken design
水平 X1转台速度/(r·min-1) X2充填深度/mm X3充填压力/kN -1 20 7 20 0 25 9 24 1 30 11 28 
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表 2 多指标综合评分法
Table 2. Multi-indices evaluation method
指标名称 评分方法 α1硬度/N 数值的0.1倍 α2脆碎度/% 数值倒数的10倍 α3崩解时间/min 数值倒数的100倍 α4片质量差异/% 数值倒数的10倍
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表 3 响应面法试验方案及结果
Table 3. Response surface design and results
序号 X1转台速度/(r·min-1) X2充填深度/mm X3充填压力/kN 片质量差异/% 硬度/N 崩解时间/min 脆碎度/% 综合评定值Y 1 -1 -1 0 2.9 53 25 0.4 18.3 2 1 -1 0 3.0 77 43 0.3 17.7 3 -1 1 0 2.5 55 26 0.4 18.9 4 1 1 0 2.0 78 43 0.3 14.6 5 -1 0 -1 1.7 59 30 0.4 16.7 6 1 0 -1 2.2 79 45 0.4 18.5 7 -1 0 1 2.7 57 26 0.4 16.9 8 1 0 1 2.5 76 40 0.1 14.1 9 0 -1 -1 1.8 64 30 0.3 19.4 10 0 1 -1 2.8 62 28 0.4 18.6 11 0 -1 1 1.8 66 35 0.4 19.2 12 0 1 1 1.6 60 28 0.2 13.8 13 0 0 0 2.5 65 30 0.3 18.7 14 0 0 0 2.1 60 31 0.4 20.1 15 0 0 0 2.4 66 37 0.3 19.7 16 0 0 0 1.8 67 38 0.3 20.0 17 0 0 0 1.7 60 31 0.4 19.2
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表 4 回归模型方程方差分析
Table 4. Analysis of variance on regression model
变异来源 平方和 自由度 均方 F值 P值 模型 60.32 9 6.70 9.26 0.0039** X1转台速度 4.35 1 4.35 6.01 0.0440* X2充填深度 9.46 1 9.46 13.08 0.0086** X3充填压力 10.58 1 10.58 14.62 0.0065** X1X2 3.42 1 3.42 4.73 0.0661 X1X3 5.29 1 5.29 7.31 0.0305* X2X3 5.29 1 5.29 7.31 0.0305* X12 11.92 1 11.92 16.47 0.0048** X22 0.98 1 0.98 1.35 0.2826 X32 7.20 1 7.20 9.95 0.0161* 残差 5.06 7 0.72 失拟项 3.69 3 1.23 3.59 0.1245 纯误差 1.37 4 0.34 总变异 65.39 16 注：*表示差异显著，P＜0.05；**表示差异极显著，P＜0.01。
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